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РецензированоEN2024

TEXTURAL ANALYSIS OF A TWO-DIMENSIONAL METAL-ORGANIC FRAMEWORK CATENA[BIS (Μ2- (+) -TARTRATE) -DIAQUA-DI-ZINC (II) TRIHYDRATE] OBTAINED FROM NITROGEN ADSORPTION.

Ahrorjon Abdullaev (Institute of General and Inorganic Chemistry, Uzbekistan Academy of Sciences, PhD student) · Yuldosh Yakubov (Institute of General and Inorganic Chemistry, Uzbekistan Academy of Sciences, doctor of chemical sciences, professor) · Aziz Ibragimov (Institute of General and Inorganic Chemistry, Uzbekistan Academy of Sciences, director of institute, doctor of chemical sciences, professor Institute of General and Inorganic Chemistry of the Academy of Sciences of the Republic of Uzbekistan. 77-a Mirzo Ulugbek Street, Tashkent)

Современные подходы и новые исследования в современной науке · 71-73 · 2024

Аннотация

Nitrogen adsorption of the compound was carried out. The sample was synthesized using the solvothermal method. Its crystalline structure was confirmed by X-ray diffraction (XRD), and its purity was determined to be 99.5% through elemental analysis. The compound was used in the form of a crystalline powder. To remove adsorbed gases and moisture, the sample was degassed at a temperature of 120°C under a vacuum of <10−3 Torr for 12 hours. Prior to adsorption measurements, the sample was purified with high-purity nitrogen. The mass of the degassed sample used for adsorption measurements was 0.100 g. Nitrogen (N2) gas with a purity of 99.999% was used as the adsorbate. Before use, the gas was dried using molecular sieves.

Доказательный фрагмент

«Nitrogen adsorption of the compound was carried out.»

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Демо-превью

Nitrogen adsorption of the compound was carried out. Полный текст публикации CiteX не хранит — доступ к первоисточнику открывается по DOI согласно лицензии издателя и выбранному плану.

DOI не указан
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Тип
Журнал
Страна
Узбекистан
Ключевые слова
adsorption measurements, sample, nitrogen, used, compound, using, crystalline
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